But this is of course still only refering to my sample. Even if we may see really strong colours except white, being it orange or yellow, the DMT may still be more than 90 % + pure. Therefore it is already a condition of superior purity. Here I wanted to check, if DMT is truly sensitive to Temperature only, or if Temperature alone is not a problem at all when UV-Light is not combined.Ĭonclusion: As told in the Observation in the 1H-NMR, the total Signal Integral of DMT is 94,62 %. 6.) 1H+13C NMR Spectra of DMT which is exposed to high Heat (100 ☌ only so far). Also I may post a longterm expure within the future.

At the end I can now finally tell how much DMT is destroyed within that exposure time given. We all know it breaks down, but here I unveiled in what dimension it will be destroyed and what is formed. 5.) 1H+13C NMR Spectra + Mass Analysis of photooxidized DMT Here I wanted to investigate WHAT is happening if you don’t store your DMT correctly. Sadly I dont have much to tell about them, but a future plan is to add a spectra of ONLY the contaminants, which are washed away by recrystallizing. I also tried to subtract the Spectra of the more pure DMT from this one to show only the Peaks of the contaminants. Of course non-pure can be non-pure in any means, so I can just share what MY impure Sample is and only what I got at that specific moment. I will incluce some little thoughts of what I think about the idea of *Jungle Spice* 4.) 1H+13C NMR Spectra + Mass Analysis of non-recrystallized DMT = with lots of impurities I wanted to use this example to show what you get, when you have this brown crude oily stuff and what you can expect in terms of DMT-content when using this. 3.) 1H+13C NMR Spectra of Jungle Spice (I posted it in the original Plant Analysis thread). I wanted to use this example to show, that even this visibly orange impure stuff is already very good in terms of purity for usage as you will see. (Predicted with Mestrenova 12.0) 2.) 1H+13C NMR Spectra of yellowish-white DMT This DMT is not perfectly pure, but what you get when you have white crystals with some yellow to brown colour. Of course the prediction is not a tool to be totally free of mistakes, but I was never disappointed by this function at all at any time, also for this work.

The content so far is: 1.) The predicted 1H/13C NMR Spectra of DMT (done with Mestrenova 12.0) This will be the base for my samples to be compared to and check what’s going on there.

Sample purity mestrenova